A hydrofluoric acid (HF)-treated soil sample was studied by C-13 NMR spectroscopy. Cross polarization (CP) Magic Angle Spinning (MAS) C-13 spectral editing and relative CP peak quantitation, obtained through variable-contact-time experiments, were used to aid the interpretation of the spectrum. The combination of these two types of experiment allowed to obtain a higher degree of detail on the composition of the sample with respect to a standard CP MAS experiment.
CP MAS 13C spectral editing and relative quantitation of a soil sample / C. FORTE; A. PIAZZI; S. PIZZANELLI; G. CERTINI. - In: SOLID STATE NUCLEAR MAGNETIC RESONANCE. - ISSN 0926-2040. - STAMPA. - 30:(2006), pp. 81-88. [10.1016/j.ssnmr.2006.03.001]
CP MAS 13C spectral editing and relative quantitation of a soil sample
CERTINI, GIACOMO
2006
Abstract
A hydrofluoric acid (HF)-treated soil sample was studied by C-13 NMR spectroscopy. Cross polarization (CP) Magic Angle Spinning (MAS) C-13 spectral editing and relative CP peak quantitation, obtained through variable-contact-time experiments, were used to aid the interpretation of the spectrum. The combination of these two types of experiment allowed to obtain a higher degree of detail on the composition of the sample with respect to a standard CP MAS experiment.
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