Attempts are made to efficiently decouple C-13 nuclei without significant loss of coherence during the application of the decoupling package. Such attempts are based on the (SE)-E-3 spin-state selection method. A newly developed double (SE)-E-3 ((DSE)-E-3) is particularly efficient for C-alpha detection for proteins as large as 480 kDa.
A method for C(alpha) direct-detection in protonless NMR / W.Bermel; I.Bertini; I.C.Felli; M.Matzapetakis; R.Pierattelli; E.C.Theil; P.Turano. - In: JOURNAL OF MAGNETIC RESONANCE. - ISSN 1090-7807. - STAMPA. - 188:(2007), pp. 301-310. [10.1016/j.jmr.2007.07.004]
A method for C(alpha) direct-detection in protonless NMR
BERTINI, IVANO;FELLI, ISABELLA CATERINA;PIERATTELLI, ROBERTA;TURANO, PAOLA
2007
Abstract
Attempts are made to efficiently decouple C-13 nuclei without significant loss of coherence during the application of the decoupling package. Such attempts are based on the (SE)-E-3 spin-state selection method. A newly developed double (SE)-E-3 ((DSE)-E-3) is particularly efficient for C-alpha detection for proteins as large as 480 kDa.
File in questo prodotto:
Non ci sono file associati a questo prodotto.
I documenti in FLORE sono protetti da copyright e tutti i diritti sono riservati, salvo diversa indicazione.
