Novel adducts of lithium hexafluoroacetylacetonato {Li(hfa)} with polyethers (monoglyme = {CH3OCH2CH2OCH3}, diglyme = {CH3O(CH2CH2O)2CH3}, triglyme = {CH3O(CH2CH2O)3CH3} and tetraglyme {CH3O(CH2CH2O)4CH3} have been synthesized through a single step reaction and characterized by FT-IR spectroscopy, 1H, and 13C NMR, single crystal X-ray diffraction studies along with thermal analysis.
Facile synthesis of novel lithium β-diketonate glyme adducts: The effect of molecular engineering on the thermal properties / Peddagopu N.; Rossi P.; Bonaccorso C.; Bartasyte A.; Paoli P.; Malandrino G.. - In: DALTON TRANSACTIONS. - ISSN 1477-9226. - STAMPA. - 49:(2020), pp. 1002-1006. [10.1039/c9dt04732h]
Facile synthesis of novel lithium β-diketonate glyme adducts: The effect of molecular engineering on the thermal properties
Rossi P.;Paoli P.;
2020
Abstract
Novel adducts of lithium hexafluoroacetylacetonato {Li(hfa)} with polyethers (monoglyme = {CH3OCH2CH2OCH3}, diglyme = {CH3O(CH2CH2O)2CH3}, triglyme = {CH3O(CH2CH2O)3CH3} and tetraglyme {CH3O(CH2CH2O)4CH3} have been synthesized through a single step reaction and characterized by FT-IR spectroscopy, 1H, and 13C NMR, single crystal X-ray diffraction studies along with thermal analysis.
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