The qualitative and quantitative determination of components of mainstream and sidestream smoke has been performed by solid-phase microextraction–gas chromatography–mass spectrometry. Several brands and types of cigarettes sold in Italy were considered: normal, mild, light, extra light, some with filter and some without. Extraction of the analytes was performed by means of solid-phase microextraction (SPME) and the optimisation of the extraction procedure was performed by experimental design, taking into consideration type of fiber polymer, exposure temperature and time. Sixty-seven components of mainstream and sidestream smoke were identified. The quantified compounds (by means of deuterium-labelled isotopologues) were benzene, toluene, p-xylene, m-xylene, pyridine, o-xylene, limonene, naphthalene, phenol and nicotine. Finally, a comparison between the chemical profile of smoke from the different cigarettes was made.

Identification and determination of mainstream and sidestream smoke components in different brands and types of cigarettes by means of solid-phase microextraction-gas cromatography-mass spectrometry / G. Pieraccini; S. Furlanetto; S. Orlandini; G. Bartolucci; I. Giannini; S. Pinzauti; G. Moneti. - In: JOURNAL OF CHROMATOGRAPHY A. - ISSN 0021-9673. - STAMPA. - 1180:(2008), pp. 138-150. [10.1016/j.chroma.2007.12.029]

Identification and determination of mainstream and sidestream smoke components in different brands and types of cigarettes by means of solid-phase microextraction-gas cromatography-mass spectrometry.

PIERACCINI, GIUSEPPE
;
FURLANETTO, SANDRA;ORLANDINI, SERENA;BARTOLUCCI, GIAN LUCA;PINZAUTI, SERGIO;MONETI, GLORIANO
2008

Abstract

The qualitative and quantitative determination of components of mainstream and sidestream smoke has been performed by solid-phase microextraction–gas chromatography–mass spectrometry. Several brands and types of cigarettes sold in Italy were considered: normal, mild, light, extra light, some with filter and some without. Extraction of the analytes was performed by means of solid-phase microextraction (SPME) and the optimisation of the extraction procedure was performed by experimental design, taking into consideration type of fiber polymer, exposure temperature and time. Sixty-seven components of mainstream and sidestream smoke were identified. The quantified compounds (by means of deuterium-labelled isotopologues) were benzene, toluene, p-xylene, m-xylene, pyridine, o-xylene, limonene, naphthalene, phenol and nicotine. Finally, a comparison between the chemical profile of smoke from the different cigarettes was made.
2008
1180
138
150
G. Pieraccini; S. Furlanetto; S. Orlandini; G. Bartolucci; I. Giannini; S. Pinzauti; G. Moneti
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Utilizza questo identificatore per citare o creare un link a questa risorsa: https://hdl.handle.net/2158/325615
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