Pseudocontact shifts (PCSs) measured by solid-state NMR spectroscopy (SS-NMR) on microcrystal-line powders of a paramagnetic metalloprotein permit NMR crystallography. Along with other restraints for SS-NMR experiments, the protein molecular structure as well as the correct crystal packing are obtained.
Solid state NMR crystallography through paramagnetic restraints / C. Luchinat; G. Parigi; E. Ravera; M. Rinaldelli. - In: JOURNAL OF THE AMERICAN CHEMICAL SOCIETY. - ISSN 0002-7863. - STAMPA. - 134:(2012), pp. 5006-5009. [10.1021/ja210079n]
Solid state NMR crystallography through paramagnetic restraints
LUCHINAT, CLAUDIO;PARIGI, GIACOMO;RAVERA, ENRICO;RINALDELLI, MAURO
2012
Abstract
Pseudocontact shifts (PCSs) measured by solid-state NMR spectroscopy (SS-NMR) on microcrystal-line powders of a paramagnetic metalloprotein permit NMR crystallography. Along with other restraints for SS-NMR experiments, the protein molecular structure as well as the correct crystal packing are obtained.
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