Great theoretical and methodological advances are pushing the limits of resolution and sensitivity in solid state NMR (SSNMR). However, sample preparation remains a critical issue for the success of an experiment. The factors affecting spectral quality in SSNMR samples are discussed, examining cases encountered in the literature and presenting new experimental data. A discussion on resolution and sensitivity in sedimented solutes is framed in this context
Practical considerations over spectral quality in solid state NMR spectroscopy of soluble proteins / Marco Fragai;Claudio Luchinat;Giacomo Parigi;Enrico Ravera. - In: JOURNAL OF BIOMOLECULAR NMR. - ISSN 0925-2738. - STAMPA. - 57:(2013), pp. 155-166. [10.1007/s10858-013-9776-0]
Practical considerations over spectral quality in solid state NMR spectroscopy of soluble proteins
FRAGAI, MARCO;LUCHINAT, CLAUDIO;PARIGI, GIACOMO;RAVERA, ENRICO
2013
Abstract
Great theoretical and methodological advances are pushing the limits of resolution and sensitivity in solid state NMR (SSNMR). However, sample preparation remains a critical issue for the success of an experiment. The factors affecting spectral quality in SSNMR samples are discussed, examining cases encountered in the literature and presenting new experimental data. A discussion on resolution and sensitivity in sedimented solutes is framed in this context
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